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Article


Title

Enhancement of Magnetic and Dielectric Properties of Ni0.25Cu0.25Zn0.50Fe2O4 Magnetic Nanoparticles through Non-Thermal Microwave Plasma Treatment for High-Frequency and Energy Storage Applications

Authors

[ 1 ] Instytut Technologii Mechanicznej, Wydział Inżynierii Mechanicznej, Politechnika Poznańska | [ P ] employee

Scientific discipline (Law 2.0)

[2.8] Mechanical engineering

Year of publication

2022

Published in

Materials

Journal year: 2022 | Journal volume: vol. 15 | Journal number: iss. 19

Article type

scientific article

Publication language

english

Keywords
EN
  • ferrite nanoparticles
  • non-thermal plasma
  • dielectric properties
  • magnetization
  • conductivity
  • energy storage
Abstract

EN Spinel ferrites are widely investigated for their widespread applications in high-frequency and energy storage devices. This work focuses on enhancing the magnetic and dielectric properties of Ni0.25Cu0.25Zn0.50 ferrite series through non-thermal microwave plasma exposure under low-pressure conditions. A series of Ni0.25Cu0.25Zn0.50 ferrites was produced using a facile sol–gel auto-ignition approach. The post-synthesis plasma treatment was given in a low-pressure chamber by sustaining oxygen plasma with a microwave source. The structural formation of control and plasma-modified ferrites was investigated through X-ray diffraction analysis, which confirmed the formation of the fcc cubical structure of all samples. The plasma treatment did not affect crystallize size but significantly altered the surface porosity. The surface porosity increased after plasma treatment and average crystallite size was measured as about ~49.13 nm. Morphological studies confirmed changes in surface morphology and reduction in particle size on plasma exposure. The saturation magnetization of plasma-exposed ferrites was roughly 65% higher than the control. The saturation magnetization, remnant magnetization, and coercivity of plasma-exposed ferrites were calculated as 74.46 emu/g, 26.35 emu/g, and 1040 Oe, respectively. Dielectric characteristics revealed a better response of plasma-exposed ferrites to electromagnetic waves than control. These findings suggest that the plasma-exposed ferrites are good candidates for constructing high-frequency devices.

Date of online publication

04.10.2022

Pages (from - to)

6890-1 - 6890-16

DOI

10.3390/ma15196890

URL

https://www.mdpi.com/1996-1944/15/19/6890

Comments

Article Number: 6890

License type

CC BY (attribution alone)

Open Access Mode

open journal

Open Access Text Version

final published version

Date of Open Access to the publication

at the time of publication

Ministry points / journal

140.0

Impact Factor

3.748 [List 2021]

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